Spatiotemporal Multitechnique Imaging of a Catalytic Solid in Action: Phase Variation and Volatilization During Molybdenum Oxide Reduction

Matthew G. O'Brien; Andrew M. Beale; Simon D. M. Jacques; Marco Di Michiel; Bert M. Weckhuysen

doi:10.1002/cctc.200900042

Spatiotemporal Multitechnique Imaging of a Catalytic Solid in Action: Phase Variation and Volatilization During Molybdenum Oxide Reduction

Matthew G. O'Brien, Andrew M. Beale, Simon D. M. Jacques, Marco Di Michiel, Bert M. Weckhuysen

Utrecht University of Applied Sciences

Research output: Contribution to journal › Article › Academic › peer-review

Abstract

Caught in the act: A novel combined experimental setup is demonstrated, which uses very high energy/flux synchrotron X-rays and allows the measurement of spatiotemporal data on larger reactors and the use of techniques such as fluorescence spectroscopy and Compton scattering. Wide-angle X-ray and Compton scattering reveal information on the causes of molybdenum volatilization in partial oxidation catalysts.

Original language	English
Pages (from-to)	99-102
Number of pages	4
Journal	ChemCatChem
Volume	1
Issue number	1
DOIs	https://doi.org/10.1002/cctc.200900042
Publication status	Published - Sept 2009

Keywords

X-ray absorption spectroscopy
Fluorescence
Molybdenum
Operando techniques
Reduction

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10.1002/cctc.200900042

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keywords = "X-ray absorption spectroscopy, Fluorescence, Molybdenum, Operando techniques, Reduction",

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year = "2009",

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AU - Weckhuysen, Bert M.

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KW - X-ray absorption spectroscopy

KW - Fluorescence

KW - Molybdenum

KW - Operando techniques

KW - Reduction

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Spatiotemporal Multitechnique Imaging of a Catalytic Solid in Action: Phase Variation and Volatilization During Molybdenum Oxide Reduction

Abstract

Keywords

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