Polystyrylboronic acid as a reusable polymeric support for oligosaccharide synthesis

G. Belogi; T. Zhu; G. J. Boons

doi:10.1016/S0040-4039(00)01184-9

Polystyrylboronic acid as a reusable polymeric support for oligosaccharide synthesis

G. Belogi, T. Zhu, G. J. Boons^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › Academic › peer-review

Abstract

Polystyrylboronic acid is an attractive polymeric support for oligosaccharide synthesis that can easily be prepared in high loading capacity and re-used after a synthetic sequence. Saccharides were loaded by heating in pyridine and released by treatment with a mixture of acetone and water. NIS/TMSOTf mediated glycosidations of thioglycosides gave a quantitative formation of disaccharides. (C) 2000 Published by Elsevier Science Ltd.

Original language	English
Pages (from-to)	6965-6968
Number of pages	4
Journal	Tetrahedron Letters
Volume	41
Issue number	36
DOIs	https://doi.org/10.1016/S0040-4039(00)01184-9
Publication status	Published - 2 Sept 2000
Externally published	Yes

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10.1016/S0040-4039(00)01184-9

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title = "Polystyrylboronic acid as a reusable polymeric support for oligosaccharide synthesis",

abstract = "Polystyrylboronic acid is an attractive polymeric support for oligosaccharide synthesis that can easily be prepared in high loading capacity and re-used after a synthetic sequence. Saccharides were loaded by heating in pyridine and released by treatment with a mixture of acetone and water. NIS/TMSOTf mediated glycosidations of thioglycosides gave a quantitative formation of disaccharides. (C) 2000 Published by Elsevier Science Ltd.",

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AU - Belogi, G.

AU - Zhu, T.

AU - Boons, G. J.

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Y1 - 2000/9/2

N2 - Polystyrylboronic acid is an attractive polymeric support for oligosaccharide synthesis that can easily be prepared in high loading capacity and re-used after a synthetic sequence. Saccharides were loaded by heating in pyridine and released by treatment with a mixture of acetone and water. NIS/TMSOTf mediated glycosidations of thioglycosides gave a quantitative formation of disaccharides. (C) 2000 Published by Elsevier Science Ltd.

AB - Polystyrylboronic acid is an attractive polymeric support for oligosaccharide synthesis that can easily be prepared in high loading capacity and re-used after a synthetic sequence. Saccharides were loaded by heating in pyridine and released by treatment with a mixture of acetone and water. NIS/TMSOTf mediated glycosidations of thioglycosides gave a quantitative formation of disaccharides. (C) 2000 Published by Elsevier Science Ltd.

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JO - Tetrahedron Letters

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Polystyrylboronic acid as a reusable polymeric support for oligosaccharide synthesis

Abstract

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