Insight into the phase transformations between ice Ih and ice II from electron backscatter diffraction data

  • D.J. Prior
  • , S. Diebold
  • , R. Obbard
  • , C. Daghlian
  • , D.L. Goldsby
  • , W.B. Durham
  • , I. Baker

Research output: Contribution to journalArticleAcademicpeer-review

Abstract

Electronbackscatterdiffractiondata from polycrystalline water ice, cycled three times through the 1h to IIphasetransformation, show that an area equivalent to the original grain size (∼450 μm) now comprises equant 10 μm grains with a non-random crystallographic preferred orientation (CPO). Pole figures show small-circle ring and fence patterns characteristic of CPO development controlled by an orientation relationship during phasetransformation. Misorientation analysis shows that one of two orientation relationships can explain the data:1h/II, {1 0-1 0}1h/{0 0 0 1}II or 1h/II, {1 0-1 0}1h/{0 0 0 1}II
Original languageEnglish
Pages (from-to)69-72
Number of pages4
JournalScripta Materialia
Volume66
Issue number2
DOIs
Publication statusPublished - 2012

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